2,2,6,6-四甲基哌啶氧化物合成路线 (共 284 条)
反应条件
in tetrahydrofuran
T=20°C; 2 h; Irradiation;
参考文献
Giese, Bernd; Gebhard, Thoma
Helvetica Chimica Acta, 1991 , vol. 74, # 5 p. 1143 - 1155
反应条件
in tetrahydrofuran; diethyl ether
T=-10°C; Title compound not separated from byproducts;
参考文献
Daikh, Brian E.; Finke, Richard G.
Journal of the American Chemical Society, 1991 , vol. 113, # 11 p. 4160 - 4172
反应条件
in toluene
T=100°C; 8 h; ΔH(excit.), ΔS(excit.); Rate constantThermodynamic data;
参考文献
Huang, Wen-Wei; Henry-Riyad, Huda; Tidwell, Thomas T.
Journal of the American Chemical Society, 1999 , vol. 121, # 16 p. 3939 - 3943
反应条件
ethylcobaloxime lt;C2H5-Co(dmgH)2Pygt; in ethanol
3 h; Irradiation;
参考文献
Brown, Trevor M.; Cooksey, Christopher J.; Crich, David; Dronsfield, Alan T.; Ellis, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2131 - 2136
反应条件
in 2,2,4-trimethylpentane
T=18°C; var. solvents; Rate constant;
参考文献
Sobek; Martschke; Fischer
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2849 - 2857
反应条件
(pyridine)Co(dimethylglyoxime)2CH3 in ethanol
18 h; Irradiation;
参考文献
Brown, Trevor M.; Cooksey, Christopher J.; Crich, David; Dronsfield, Alan T.; Ellis, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2131 - 2136
反应条件
in benzene
T=110°C; 24 h;
参考文献
Merkley; Venneri; Warkentin
Canadian Journal of Chemistry, 2001 , vol. 79, # 3 p. 312 - 318
反应条件
(t-BuO)2
Irradiation;
参考文献
Connolly, Terrence J.; Baldovi; Mohtat; Scaiano
Tetrahedron Letters, 1996 , vol. 37, # 28 p. 4919 - 4922
反应条件
in hexane
0.0833333 h; IrradiationRayonet reactor;
参考文献
Korolenko, E. C.; Cozens, F. L.; Scaiano, J. C.
Journal of Physical Chemistry, 1995 , vol. 99, # 38 p. 14123 - 14128
反应条件
in benzene
T=100°C; Ring cleavage; 96 h; Thermolysis; Product distributionKinetics;
参考文献
Merkley, Nadine; El-Saidi, Manal; Warkentin, John
Canadian Journal of Chemistry, 2000 , vol. 78, # 3 p. 356 - 361