2,2,6,6-四甲基哌啶氧化物合成路线 （共 284 条）
反应条件
sodium tetrahydroborate; Fe2(ox)3.6H2O in water; acetonitrile
T=0°C; 0.583333 h; Inert atmosphere;
参考文献
Ishikawa, Hayato; Colby, David A.; Seto, Shigeki; Va, Porino; Tam, Annie; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 4904 - 4916
反应条件
caesium carbonate in water; acetonitrile
T=25°C; 24 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Ji, Guojing; Wang, Xi; Zhang, Songnan; Xu, Yan; Ye, Yuxuan; Li, Ming; Zhang, Yan; Wang, Jianbo
Chemical Communications, 2014 , vol. 50, # 33 p. 4361 - 4363
反应条件
1: C15H16O With Co(3-Me-5-MeO-salen) in acetonitrile
T=-20 - 20°C; 0.166667 h; Inert atmosphere;
2: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical With dihydrogen peroxide in water; acetonitrile
T=-20°C; 24 h; Inert atmosphere;
3: With hydrogenchloride in water; acetonitrile
T=0 - 20°C; 0.25 h; Inert atmosphere;
参考文献
Watanabe, Eiichi; Kaiho, Atsushi; Kusama, Hiroyuki; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11744 - 11747
反应条件
magnesium in diethyl ether
T=34°C;
参考文献
Lawrence, Lynnette M.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2493 - 2494
反应条件
magnesium in diethyl ether
T=34°C; other reagens, reagens ratio; Product distribution;
参考文献
Lawrence, Lynnette M.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2493 - 2494
反应条件
in diethyl ether
T=34°C; other reagens, reagens ratio, mode of addition; Product distribution;
参考文献
Lawrence, Lynnette M.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2493 - 2494
反应条件
potassium carbonate; 1-tert-butylperoxy-1,2-benziodoxol-3(1H)-one in cyclohexane
72 h; Ambient temperature;
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
sodium tetrahydroborate; Mn(salen)Cl in isopropyl alcohol
24 h;
参考文献
Cai, Huanhuan; Jiang, Guoliang; Shen, Zhihao; Fan, Xinghe
Macromolecules, 2012 , vol. 45, # 15 p. 6176 - 6184
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1H-1,2,4-triazol-4-ium iodide in tetrahydrofuran
T=20°C; 6 h; Inert atmosphere;
参考文献
Guin, Joyram; De Sarkar, Suman; Grimme, Stefan; Studer, Armido
Angewandte Chemie - International Edition, 2008 , vol. 47, # 45 p. 8727 - 8730
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1H-1,2,4-triazol-4-ium iodide in tetrahydrofuran
T=20°C; 6 h; Inert atmosphere;
参考文献
Guin, Joyram; De Sarkar, Suman; Grimme, Stefan; Studer, Armido
Angewandte Chemie - International Edition, 2008 , vol. 47, # 45 p. 8727 - 8730
