2,2,6,6-四甲基哌啶氧化物合成路线 (共 284 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1H-1,2,4-triazol-4-ium iodide
T=20°C; Inert atmosphere;
参考文献
Guin, Joyram; De Sarkar, Suman; Grimme, Stefan; Studer, Armido
Angewandte Chemie - International Edition, 2008 , vol. 47, # 45 p. 8727 - 8730
反应条件
sulfuric acid in water
T=80°C; KineticsMechanism; Temperature;
参考文献
Ma, Yun; Loyns, Colin; Price, Peter; Chechik, Victor
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5573 - 5578
反应条件
dipotassium peroxodisulfate; trifluoroacetic acid
T=20°C; 24 h; Inert atmosphere;
参考文献
More, Nagnath Yadav; Jeganmohan, Masilamani
Organic Letters, 2014 , vol. 16, # 3 p. 804 - 807
反应条件
tris-(trimethylsilyl)silane in benzene
T=80°C; 3 h; other reagents, reaction time, solvent, effect of irradiation and addition of initiators; Product distributionMechanism;
参考文献
Lucarini, Marco; Marchesi, Emanuela; Pedulli, Gian Franco; Chatgilialoglu, Chryssostomos
Journal of Organic Chemistry, 1998 , vol. 63, # 5 p. 1687 - 1693
反应条件
in benzene
T=70°C; Product distributionKinetics; Further Variations:Temperatures;
参考文献
Kin, Shing Chan; Xin, Zhu Li; Dzik, Wojciech I.; De Bruin, Bas
Journal of the American Chemical Society, 2008 , vol. 130, # 6 p. 2051 - 2061
反应条件
in acetonitrile-D3
T=24.84°C; Inert atmosphere; Equilibrium constant; SolventTemperature;
参考文献
Wu, Adam; Mader, Elizabeth A.; Datta, Ayan; Hrovat, David A.; Borden, Weston Thatcher; Mayer, James M.
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11985 - 11997
反应条件
in acetonitrile-D3
T=24.84°C; Inert atmosphere; Equilibrium constant; SolventTemperature;
参考文献
Wu, Adam; Mader, Elizabeth A.; Datta, Ayan; Hrovat, David A.; Borden, Weston Thatcher; Mayer, James M.
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11985 - 11997
反应条件
in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Khaskin, Eugene; Diskin-Posner, Yael; Weiner, Lev; Leitus, Gregory; Milstein, David
Chemical Communications, 2013 , vol. 49, # 27 p. 2771 - 2773
反应条件
in benzene-d6
Inert atmosphere;
参考文献
Dikanov, S. A.; Grigor'ev, I. A.; Volodarskii, L. B.; Tsvetkov, Yu. D.
Russian Journal of Physical Chemistry, 1982 , vol. 56, # 11 p. 1696 - 1699
Zhurnal Fizicheskoi Khimii, 1982 , vol. 56, # 11 p. 2762 - 2767
反应条件
in ethanol
T=20°C; 0.5 h; titration of other nitroxide free radicals by nuclear magnetic relaxometry;
参考文献
Muller, Robert N.; Van Haverbeke, Yves; Bonnet, Pierre A.; Chapat, Jean-Pierre; Vallet, Patrick
Analytical Chemistry, 1990 , vol. 62, # 15 p. 1671 - 1673