N-苯甲酰-L-苯基丙氨酸合成路线 (共 71 条)
反应条件
1: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane 2: hydrogenchloride; orthoformic acid triethyl ester; sulfuric acid 3: palladium hydroxide on carbon; hydrogen / ethanol 4: triethylamine / dichloromethane 5: hydrogenchloride / tetrahydrofuran; water / 0 °C View Scheme
参考文献
RSC Advances, , vol. 4, # 5 p. 2389 - 2392
反应条件
1: hydrogenchloride; orthoformic acid triethyl ester; sulfuric acid 2: palladium hydroxide on carbon; hydrogen / ethanol 3: triethylamine / dichloromethane 4: hydrogenchloride / tetrahydrofuran; water / 0 °C View Scheme
参考文献
RSC Advances, , vol. 4, # 5 p. 2389 - 2392
反应条件
1: palladium hydroxide on carbon; hydrogen / ethanol 2: triethylamine / dichloromethane 3: hydrogenchloride / tetrahydrofuran; water / 0 °C View Scheme
参考文献
RSC Advances, , vol. 4, # 5 p. 2389 - 2392
反应条件
1: hydrogenchloride / tetrahydrofuran; water / 0 °C View Scheme
参考文献
RSC Advances, , vol. 4, # 5 p. 2389 - 2392
反应条件
1.1: C24H34N2O2; N-(2-hydroxybenzyl)amine / toluene / 72 h / |Reflux 1.2: 20 °C 2.1: triethylamine / dichloromethane 3.1: hydrogenchloride / tetrahydrofuran; water / 0 °C View Scheme
参考文献
RSC Advances, , vol. 4, # 5 p. 2389 - 2392
反应条件
1: NaOH / H2O / 2 h / 20 °C 2: corn steep liquor; fungus Beauveria bassiana ATCC 7159; glucose / ethanol; H2O / 72 h / Enzymatic reaction View Scheme
参考文献
Monatshefte fur Chemie, , vol. 131, # 6 p. 667 - 672
反应条件
1: NaOH / H2O / 2 h / 20 °C 2: corn steep liquor; fungus Beauveria bassiana ATCC 7159; glucose / ethanol; H2O / 72 h / Enzymatic reaction View Scheme
参考文献
Monatshefte fur Chemie, , vol. 131, # 6 p. 667 - 672
反应条件
D-glucose; corn steep liquor; fungus Beauveria bassiana ATCC 7159 in ethanol; water Hydrolysis; 72 h; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Monatshefte fur Chemie, , vol. 131, # 6 p. 667 - 672
反应条件
1.1: sodium hydroxide / water / 20 °C 1.2: 2 h / pH 2 2.1: acetic anhydride / 2 h / 65 °C 3.1: Candida antarctica B lipase; water / acetonitrile / 72 h / 37 °C / Enzymatic reaction View Scheme
参考文献
Chemical Communications, , vol. 48, # 37 p. 4411 - 4413
反应条件
1: acetic anhydride / 2 h / 65 °C 2: Candida antarctica B lipase; water / acetonitrile / 72 h / 37 °C / Enzymatic reaction View Scheme
参考文献
Chemical Communications, , vol. 48, # 37 p. 4411 - 4413