4,7-二氢-2-苯基-1,3-二氧杂环庚合成路线 (共 6 条)
参考文献
Soulie, J.; Lampilas, M.; Lallemand, J. Y.
Tetrahedron, 1987 , vol. 43, # 12 p. 2701 - 2708
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one; orthoformic acid triethyl ester in ethanol T=50°C; 7 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Shaterian, Hamid Reza
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 10 p. 2195 - 2205
反应条件
in tetrahydrofuran 1.) -78 deg C, 1 h, 2.) 20 deg C, 1 h;
参考文献
Demailly; Ousset; Mioskowski
Tetrahedron Letters, 1984 , vol. 25, # 41 p. 4647 - 4650
反应条件
lithium aluminium tetrahydride
参考文献
Naruta, Yoshinori; Nagai, Naoshi; Maruyama, Kazuhiro
Chemistry Letters, 1983 , p. 1383 - 1386
反应条件
triethylamine in toluene
T=50°C; 48 h;
参考文献
Timpe, H.-J.; Schmidt, M.; Fisera, L'.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 5 p. 735 - 747
反应条件
triethylamine in diethyl ether
T=0 - 5°C; 1 h;
参考文献
Camilleri, Patrick; Munro, David; Weaver, Karen; Williams, David J.; Rzepa, Henry S.; Slawin, Alexandra M. Z.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1929 - 1934