2-丙基噻唑并[4,5-c]喹啉-4-胺合成路线 （共 7 条）
反应条件
ammonium hydroxide in chloroform
参考文献
3M Innovative Properties Company
Patent: US6110929 A1, 2000 ;
参考文献
3M Innovative Properties Company
Patent: US6110929 A1, 2000 ;
反应条件
1: With benzoyl isocyanate in dichloromethane 0.5 h; Reflux; 2: With sodium methylate in methanol 2 h; Reflux;
参考文献
Kokatla, Hari Prasad; Yoo, Euna; Salunke, Deepak B.; Sil, Diptesh; Ng, Cameron F.; Balakrishna, Rajalakshmi; Malladi, Subbalakshmi S.; Fox, Lauren M.; David, Sunil A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 7 p. 1179 - 1198
反应条件
1.1: pyridine; tetraphosphorus decasulfide / 2 h / |Reflux 2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 20 °C 3.1: benzoyl isocyanate / dichloromethane / 0.5 h / |Reflux 3.2: 2 h / |Reflux View Scheme
参考文献
Kokatla, Hari Prasad; Yoo, Euna; Salunke, Deepak B.; Sil, Diptesh; Ng, Cameron F.; Balakrishna, Rajalakshmi; Malladi, Subbalakshmi S.; Fox, Lauren M.; David, Sunil A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 7 p. 1179 - 1198
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 20 °C 2.1: benzoyl isocyanate / dichloromethane / 0.5 h / |Reflux 2.2: 2 h / |Reflux View Scheme
参考文献
Kokatla, Hari Prasad; Yoo, Euna; Salunke, Deepak B.; Sil, Diptesh; Ng, Cameron F.; Balakrishna, Rajalakshmi; Malladi, Subbalakshmi S.; Fox, Lauren M.; David, Sunil A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 7 p. 1179 - 1198
反应条件
1.1: acetic anhydride; sodium acetate / 0.25 h / |Reflux 2.1: hydrogen; platinum on carbon / N,N-dimethyl-formamide / 3.5 h / 3102.97 Torr 3.1: triethylamine / N,N-dimethyl-formamide; dichloromethane / 0 °C 4.1: pyridine; tetraphosphorus decasulfide / 2 h / |Reflux 5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 20 °C 6.1: benzoyl isocyanate / dichloromethane / 0.5 h / |Reflux 6.2: 2 h / |Reflux View Scheme
参考文献
Kokatla, Hari Prasad; Yoo, Euna; Salunke, Deepak B.; Sil, Diptesh; Ng, Cameron F.; Balakrishna, Rajalakshmi; Malladi, Subbalakshmi S.; Fox, Lauren M.; David, Sunil A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 7 p. 1179 - 1198
反应条件
1.1: hydrogen; platinum on carbon / N,N-dimethyl-formamide / 3.5 h / 3102.97 Torr 2.1: triethylamine / N,N-dimethyl-formamide; dichloromethane / 0 °C 3.1: pyridine; tetraphosphorus decasulfide / 2 h / |Reflux 4.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 20 °C 5.1: benzoyl isocyanate / dichloromethane / 0.5 h / |Reflux 5.2: 2 h / |Reflux View Scheme
参考文献
Kokatla, Hari Prasad; Yoo, Euna; Salunke, Deepak B.; Sil, Diptesh; Ng, Cameron F.; Balakrishna, Rajalakshmi; Malladi, Subbalakshmi S.; Fox, Lauren M.; David, Sunil A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 7 p. 1179 - 1198
