4-(1H-1,2,4-噻唑-1-基)苯甲腈合成路线 （共 3 条）
反应条件
2,3'-bipyridine; ammonium hydroxide; copper(l) iodide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen in ethanol
T=20°C; 24 h;
参考文献
Yin, Weiyu; Wang, Chengming; Huang, Yong
Organic Letters, 2013 , vol. 15, # 8 p. 1850 - 1853
反应条件
8-Hydroxyquinoline 1-oxide; caesium carbonate; copper(I) bromide in dimethyl sulfoxide
T=110°C; Ullmann coupling; 26 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Yang, Kai; Qiu, Yatao; Li, Zheng; Wang, Zhaoyang; Jiang, Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3151 - 3159
反应条件
8-Hydroxyquinoline 1-oxide; caesium carbonate; copper(I) bromide in dimethyl sulfoxide
T=110°C; Ullmann coupling; 20 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Yang, Kai; Qiu, Yatao; Li, Zheng; Wang, Zhaoyang; Jiang, Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3151 - 3159
