2,4,6-三甲基苯甲腈合成路线 (共 81 条)
反应条件
1: NH3 2: NaOH / 290 - 310 °C / 20 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 79, p. 2530
反应条件
pyridine; hydroxylamine hydrochloride 0.75 h; Heating;
参考文献
Belen'kii; Brokhovetskii; Krayushkin
Tetrahedron, 1991 , vol. 47, # 3 p. 447 - 456
反应条件
T=520 - 550°C; P=0.01 Torr;
参考文献
Meier, Michael; Ruechardt, Christoph
Chemische Berichte, 1987 , vol. 120, p. 1 - 4
反应条件
in ethanol; water T=25°C; controlled pot. electrolysis at -0.70 V, var.: solvent DMF; Mechanism;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 32, # 10 p. 3830 - 3839
反应条件
in toluene Addition; fragmentation; 2 h; Heating;
参考文献
Quadrelli; Campari; Mella; Caramella
Tetrahedron Letters, 2000 , vol. 41, # 12 p. 2019 - 2022
反应条件
aluminium trichloride in carbon disulfide
参考文献
Tetrahedron, , vol. 35, p. 2927 - 2929
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran T=0°C; 4 h; other LDA-conc.; without HMPT; also with CH3I or BuLi; Product distribution;
参考文献
Chemische Berichte, , vol. 121, p. 1159 - 1164
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran T=0°C; 4 h; other LDA-conc.; other temp; further 1,3-dithiolan-1,1-dioxide; Product distribution;
参考文献
Chemische Berichte, , vol. 121, p. 1159 - 1164
反应条件
naphthalenyl-1-carbonitrile in water; acetonitrile 36 h; Irradiation;
参考文献
Yasuda, Masahide; Pac, Chyondgjin; Sakurai, Hiroshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 746 - 750
反应条件
aluminium trichloride in nitromethane
参考文献
Bulletin of the Chemical Society of Japan, , vol. 48, p. 2607 - 2608