反应条件
1: 1.) n-BuLi / 1.) diethyl ether, n-hexane, reflux, 2.) diethyl ether, n-hexane, reflux, overnight
2: N2O4, sodium acetate / CCl4 / 1 h / 5 - 10 °C
3: LiAlH4 / diethyl ether / -30 - -10 °C
4: oxygen / benzene / 20 °C / Irradiation
View Scheme
参考文献
Tomioka, Hideo; Okada, Hidetsumu; Watanabe, Tetsuya; Banno, Kohji; Komatsu, Kazunori; Hirai, Katsuyuki
Journal of the American Chemical Society, 1997 , vol. 119, # 7 p. 1582 - 1593
