2-氨基-7-乙基-4(1H)-蝶啶酮合成路线 (共 6 条)
反应条件
sodium hydrogencarbonate; ethanethiolic acid in ethanol T=100°C; 2 h;
参考文献
Zav'yalov, S. I.; Ezhova, G. I.; Budkova, T. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 7 p. 1459 - 1462
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 7 p. 1590 - 1593
反应条件
sodium hydrogensulfite; sodium sulfite in water T=20°C; 120 h; pH = 7; Yield given. Yields of byproduct given;
参考文献
Waring; Armarego
European Journal of Medicinal Chemistry, 1987 , vol. 22, # 2 p. 83 - 90
反应条件
piperidine T=20°C; 150 h;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.; Ezhova, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 11 p. 2183 - 2185
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 11 p. 2626 - 2628
反应条件
piperidine; acetic acid 1.) 20 deg C, 145 h, 2.) 20 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.; Kravchenko, N. E.; Ezhova, G. I.; Sitkareva, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2524 - 2527
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2756 - 2759
反应条件
Yield given. Multistep reaction;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.; Kravchenko, N. E.; Ezhova, G. I.; Sitkareva, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2524 - 2527
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2756 - 2759
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.; Kravchenko, N. E.; Ezhova, G. I.; Sitkareva, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2524 - 2527
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2756 - 2759