反应条件
1.1: triethylamine / dichloromethane / 0 - 20 °C
2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C
2.2: 0 - 20 °C
3.1: [Ni0(1,5-cyclooctadiene)2]; dimethyl zinc; tri-cyclo-hexyl-phosphine / ethylene glycol dimethyl ether; toluene / 12 h / 40 °C / Inert atmosphere
View Scheme
参考文献
Hu, Jin-Xiu; Wu, Hao; Li, Chuan-Ying; Sheng, Wei-Jian; Jia, Yi-Xia; Gao, Jian-Rong
Chemistry - A European Journal, 2011 , vol. 17, # 19 p. 5234 - 5237