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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-癸基吗啉
合成路线
（共 12 条）
5299-65-0
N-癸酰基吗啡啉
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
lithium aluminium tetrahydride; sulfuric acid in tetrahydrofuran T=0°C;
参考文献
Kiuchi; Nishizawa; Kawanishi; Kinoshita; Ohsima; Uchitani; Sekino; Ishida; Kondo; Tsuda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 12 p. 3234 - 3244
31866-75-8
4-己基吗啉
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 78 percent / phenyl chloroformate / benzene / Heating 2: 1.) Mg 3: 84 percent / phenyl chloroformate / benzene / Heating 4: 1.) Mg 5: 93 percent / phenyl chloroformate / benzene / Heating 6: 1.) Mg 7: 93 percent / phenyl chloroformate / benzene / Heating 8: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
13063-60-0
4-辛基吗啉
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 93 percent / phenyl chloroformate / benzene / Heating 2: 1.) Mg 3: 93 percent / phenyl chloroformate / benzene / Heating 4: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
543-59-9
1-氯戊烷
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 1.) Mg 2: 78 percent / phenyl chloroformate / benzene / Heating 3: 1.) Mg 4: 84 percent / phenyl chloroformate / benzene / Heating 5: 1.) Mg 6: 93 percent / phenyl chloroformate / benzene / Heating 7: 1.) Mg 8: 93 percent / phenyl chloroformate / benzene / Heating 9: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
629-06-1
1-氯庚烷
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 1.) Mg 2: 93 percent / phenyl chloroformate / benzene / Heating 3: 1.) Mg 4: 93 percent / phenyl chloroformate / benzene / Heating 5: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
111-85-3
正辛基氯
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 1.) Mg 2: 93 percent / phenyl chloroformate / benzene / Heating 3: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
544-10-5
1-氯己烷
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 1.) Mg 2: 84 percent / phenyl chloroformate / benzene / Heating 3: 1.) Mg 4: 93 percent / phenyl chloroformate / benzene / Heating 5: 1.) Mg 6: 93 percent / phenyl chloroformate / benzene / Heating 7: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
82394-18-1
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 84 percent / phenyl chloroformate / benzene / Heating 2: 1.) Mg 3: 93 percent / phenyl chloroformate / benzene / Heating 4: 1.) Mg 5: 93 percent / phenyl chloroformate / benzene / Heating 6: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
82394-19-2
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
1: 93 percent / phenyl chloroformate / benzene / Heating 2: 1.) Mg View Scheme
参考文献
Yankep, Emmanuel; Charles, Georges
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 427 - 430
110-91-8
吗啉
+
124-11-8
壬烯
+
107-31-3
甲酸甲酯
→
反应条件
25727-94-0
4-癸基吗啉
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)]; tri-ruthenium(0)dodecacarbonyl; water; triphenylphosphine in N,N-dimethyl-formamide T=170°C; 6 h; AutoclaveGreen chemistry; TemperatureTime;
参考文献
Karakhanov, Eduard; Maksimov, Anton; Kardasheva, Yulia; Runova, Elena; Zakharov, Roman; Terenina, Maria; Kenneally, Corey; Arredondo, Victor
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 540 - 547
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