2,6-双-(4-甲氧基苯基)-四氢硫代吡喃-4-酮合成路线 (共 3 条)
反应条件
dipotassium hydrogenphosphate; sodium hydrogensulfide in water; isopropyl alcohol Ambient temperature;
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673
反应条件
1: 95 percent / aq. NaOH / ethanol / 15 h / Ambient temperature 2: 86 percent / K2HPO4, NaHS*2H2O / propan-2-ol; H2O / Ambient temperature View Scheme
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673
反应条件
1: 85 percent / peracetic acid / ethyl acetate; acetic acid / 1 h / Ambient temperature
2: 5 percent / I2, DMSO, H2SO4 / 2 h / 100 °C
View Scheme
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673