2,5-二苯基-4-噁唑羧酸甲酯合成路线 （共 26 条）
反应条件
silver(I) acetate; palladium diacetate; trifluoroacetic acid in 1-methyl-pyrrolidin-2-one T=120°C; Heck Reaction; 24 h; Inert atmosphereSchlenk technique;
参考文献
Li, Ziyuan; Zhou, Haipin; Xu, Jinyi; Wu, Xiaoming; Yao, Hequan
Tetrahedron, 2013 , vol. 69, # 15 p. 3281 - 3286
反应条件
silver(I) acetate; palladium diacetate; trifluoroacetic acid in 1-methyl-pyrrolidin-2-one T=120°C; Heck Reaction; 48 h; Inert atmosphereSchlenk technique; ConcentrationReagent/catalystSolventTemperatureTime;
参考文献
Li, Ziyuan; Zhou, Haipin; Xu, Jinyi; Wu, Xiaoming; Yao, Hequan
Tetrahedron, 2013 , vol. 69, # 15 p. 3281 - 3286
反应条件
N-bromosuccinmide in 1,2-dichloro-ethane T=100°C; 12 h; Reagent/catalyst;
参考文献
Bathula, Surendar Reddy; Reddy, Muktapuram Prathap; Viswanadham, K. K. Durga Rao; Sathyanarayana, Pochampalli; Reddy, Maddi Sridhar
European Journal of Organic Chemistry, 2013 , # 21 p. 4552 - 4557
反应条件
PdCl2(MeCN)2; water; copper(ll) bromide in dimethyl sulfoxide T=100°C; 8 h; regioselective reaction;
参考文献
Zheng, Jia; Zhang, Min; Huang, Liangbin; Hu, Xiaohan; Wu, Wanqing; Huang, Huawen; Jiang, Huangfeng
Chemical Communications, 2014 , vol. 50, # 27 p. 3609 - 3611
反应条件
N-bromosuccinmide in tetrachloromethane T=100°C; 24 h; SolventTimeReagent/catalyst;
参考文献
Bathula, Surendar Reddy; Reddy, Muktapuram Prathap; Viswanadham, K. K. Durga Rao; Sathyanarayana, Pochampalli; Reddy, Maddi Sridhar
European Journal of Organic Chemistry, 2013 , # 21 p. 4552 - 4557
反应条件
silver(I) acetate; palladium diacetate; 2,2,2-trimethylacetic acid T=120°C; 12 h;
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid T=120°C; 12 h;
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
1: bis(2-methoxyethyl)aminosulfur trifluoride / CH2Cl2 / 0.5 h / -20 °C 2: BrCCl3; DBU / CH2Cl2 / 8 h / 2 - 3 °C View Scheme
参考文献
Phillips; Uto; Wipf; Reno; Williams
Organic letters, 2000 , vol. 2, # 8 p. 1165 - 1168
反应条件
1: potassium carbonate / 20 °C 2: bromine; calcium carbonate / chloroform / 0 - 20 °C 3: caesium carbonate; copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride / 1,4-dioxane / 80 °C / |Inert atmosphere View Scheme
参考文献
Liu, Bingjie; Zhang, Yueteng; Huang, Gang; Zhang, Xinting; Niu, Pengfei; Wu, Jie; Yu, Wenquan; Chang, Junbiao
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 23 p. 3912 - 3923
反应条件
1: bromine; calcium carbonate / chloroform / 0 - 20 °C 2: caesium carbonate; copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride / 1,4-dioxane / 80 °C / |Inert atmosphere View Scheme
参考文献
Liu, Bingjie; Zhang, Yueteng; Huang, Gang; Zhang, Xinting; Niu, Pengfei; Wu, Jie; Yu, Wenquan; Chang, Junbiao
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 23 p. 3912 - 3923
