2,5-二苯基-4-噁唑羧酸甲酯合成路线 （共 26 条）
反应条件
1: hydroxylamine hydrochloride; sodium carbonate / methanol; water / Reflux 2: acetic anhydride / Reflux 3: hydrogenchloride / 0 - 20 °C 4: triethylamine / dichloromethane / 0 - 20 °C 5: copper diacetate / N,N-dimethyl-formamide / 120 °C 6: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
1: hydrogenchloride / 0 - 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C 3: copper diacetate / N,N-dimethyl-formamide / 120 °C 4: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
1: acetic anhydride / Reflux 2: hydrogenchloride / 0 - 20 °C 3: triethylamine / dichloromethane / 0 - 20 °C 4: copper diacetate / N,N-dimethyl-formamide / 120 °C 5: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
1: copper diacetate / N,N-dimethyl-formamide / 120 °C 2: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
1.1: water; potassium hydroxide / methanol / 3 h / 60 °C 1.2: 0 °C / pH 2 2.1: acetic acid; silver carbonate / dimethyl sulfoxide / 24 h / 120 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.166667 h; 2: With water in tetrahydrofuran T=0°C;
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
