N,N-二甲基-4-(三氟甲基)苯甲酰胺合成路线 （共 11 条）
反应条件
sodium iodide in dimethyl sulfoxide T=20°C; Electrochemical reaction;
参考文献
Huang, Haolai; Yuan, Gaoqing; Li, Xianwei; Jiang, Huanfeng
Tetrahedron Letters, 2013 , vol. 54, # 52 p. 7156 - 7159
反应条件
potassium carbonate in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; EBEL, Heiner; FRATTINI, Sara; GIOVANNINI, Riccardo; HOENKE, Christoph; SCHEUERER, Stefan
Patent: WO2011/147772 A1, 2011 ;
Location in patent: Page/Page column 86 ;
WO 2011/147772 A1
反应条件
trichlorophosphate; tris(dibenzylideneacetone)dipalladium (0) T=120°C; 24 h;
参考文献
Hosoi, Kazushi; Nozaki, Kyoko; Hiyama, Tamejiro
Organic Letters, 2002 , vol. 4, # 17 p. 2849 - 2851
反应条件
potassium carbonate in tetrahydrofuran T=0 - 20°C; 18 h; Inert atmosphere;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; EBEL, Heiner; FRATTINI, Sara; GERLACH, Kai; GIOVANNINI, Riccardo; HOENKE, Christoph; MAZZAFERRO, Rocco; SANTAGOSTINO, Marco; SCHEUERER, Stefan; TAUTERMANN, Christofer; TRIESELMANN, Thomas
Patent: WO2011/73154 A1, 2011 ;
Location in patent: Page/Page column 129 ;
WO 2011/073154 A1
反应条件
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrachloromethane; water T=20°C; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Synlett, 2012 , vol. 23, # 8 p. 1175 - 1180
反应条件
tert.-butylhydroperoxide; Cu(ClO4)2*6H2O T=100°C; 6 h;
参考文献
Kumar, P. Santhosh; Kumar, G. Sathish; Kumar, R. Arun; Reddy, N. Veera; Rajender Reddy
European Journal of Organic Chemistry, 2013 , # 7 p. 1218 - 1222
反应条件
hydrogenchloride; tert.-butylhydroperoxide; iodine in cyclohexane; water T=70 - 80°C; 20 h;
参考文献
Gao, Lingfeng; Tang, Haoming; Wang, Zhiyong
Chemical Communications, 2014 , vol. 50, # 31 p. 4085 - 4088
反应条件
tert.-butylhydroperoxide; iodine; sodium hydroxide T=70 - 80°C; 24 h;
参考文献
Xu, Kun; Hu, Yanbin; Zhang, Sheng; Zha, Zhenggen; Wang, Zhiyong
Chemistry - A European Journal, 2012 , vol. 18, # 32 p. 9793 - 9797
反应条件
copper(I) oxide; 1,10-phenanthroline; oxygen; toluene-4-sulfonic acid T=140°C; P=760.051 Torr; 24 h; Sealed tube;
参考文献
Hu, Chenxu; Yan, Xufei; Zhou, Xiangge; Li, Zhengkai
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 47 p. 8179 - 8182
反应条件
[Pt(divinyltetramethyldisiloxane)2(N,N'-di(tert-butyl)imidazol-2-ylidene)]; (Ph)2SiH2 in tetrahydrofuran; α-n-hexadecene
T=40°C; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Pisiewicz, Sabine; Junge, Kathrin; Beller, Matthias
European Journal of Inorganic Chemistry, 2014 , # 14 p. 2345 - 2349
