四-(4-氟苯基)硼化钠水合物合成路线 (共 8 条)
反应条件
1: With magnesium; ethylene dibromide in diethyl ether T=20°C; 1.5 h; Inert atmosphere; 2: With sodium tetrafluoroborate in diethyl ether T=20°C; 32 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 22 p. 3795 - 3798
反应条件
sodium chloride in diethyl ether; water pouring the reaction mixture into ice-cold satd. aq. NaCl soln.; extrn. with ether; addn. of xylene and removing the ether;
参考文献
Analytica Chimica Acta, , vol. 35, p. 1 - 5
B: B-Verb.8, 11.2.3, page 167 - 173
US3468959 , ;
C.A., , vol. 71, p. 126670
参考文献
B: B-Verb.8, 11.2.3, page 167 - 173
US3468959 , ;
C.A., , vol. 71, p. 126670
反应条件
tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=80°C; 5 h; Title compound not separated from byproducts;
参考文献
Gazzetta Chimica Italiana, , vol. 120, p. 779 - 781
反应条件
tetrakis(triphenylphosphine) palladium(0) in various solvent(s)
T=80°C; 5 h; Title compound not separated from byproducts;
参考文献
Catellani, Marta; Chiusoli, Gian Paolo; Fornasari, Vilma
Gazzetta Chimica Italiana, 1990 , vol. 120, p. 779 - 781
反应条件
vesicles(liposomes) of [3,5-didodecyl-2,6-bis{N-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}methylphenyl)iminomethyl}phenyl]chloropalladium in water
T=25°C; Miyaura-Michael reaction; 12 h; shaking;
参考文献
Hamasaka, Go; Muto, Tsubasa; Uozumi, Yasuhiro
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4876 - 4878
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.166667 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641