3-(2-羟基-乙氧基)-苯甲酸合成路线 （共 2 条）
反应条件
1: 2-(3-chlorophenoxy)ethanol With n-butyllithium; Mg(OCH2CH2OEt)2 in tetrahydrofuran T=-78°C; deprotonation; 0.25 h; 2: With Li-naphthalenide in tetrahydrofuran T=-78 - -50°C; lithium-halogen exchange; 0.333333 h; 3: carbon dioxide in tetrahydrofuran; diethyl ether Carboxylation;
参考文献
Salteris, Constantinos S.; Kostas, Ioannis D.; Micha-Screttas, Maria; Steele, Barry R.; Heropoulos, George A.; Screttas, Constantinos G.; Terzis, Aris
Journal of Organometallic Chemistry, 1999 , vol. 590, # 1 p. 63 - 70
参考文献
Ujiie, Seiji; Maekawa, Kazuhiko; Takahashi, Satoshi; Iimura, Kazuyoshi
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1993 , vol. 237, p. 477 - 482
