4-氨基-alpha-苯基苄醇合成路线 (共 6 条)
反应条件
calcium chloride; zinc in ethanol; water T=80°C; 3 h;
参考文献
Yasuda; Onishi; Ueba; Miyai; Baba
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7741 - 7744
反应条件
sodium tetrahydroborate in methanol T=20°C; 1 h;
参考文献
Gomaa, Mohamed Sayed; Armstrong, Jane L.; Bobillon, Beatrice; Veal, Gareth J.; Brancale, Andrea; Redfern, Christopher P.F.; Simons, Claire
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 17 p. 8301 - 8313
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Conover; Tarbell
Journal of the American Chemical Society, 1950 , vol. 72, p. 3586
反应条件
1: 30 percent / NaBH4 / ethanol / 0.83 h / 0 °C 2: 76 percent / zinc; calcium chloride / ethanol; H2O / 3 h / 80 °C View Scheme
参考文献
Yasuda; Onishi; Ueba; Miyai; Baba
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7741 - 7744
参考文献
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1920 , vol. 39, p. 493
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=80°C; 21 h; optical yield given as percent ee;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 4 p. 497 - 502