(4-氯苯基硫)丙-2-酮合成路线 (共 14 条)
反应条件
FeBr2 in tetrahydrofuran T=20°C; 24 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 23 p. 6124 - 6130
参考文献
Journal of Medicinal Chemistry, , vol. 31, # 5 p. 954 - 959
反应条件
in various solvent(s) 2 h;
参考文献
Enantiomer, , vol. 7, # 4-5 p. 231 - 240
反应条件
potassium permanganate; acetic acid
参考文献
Ohta; Sudoh
Yakugaku Zasshi, 1949 , vol. 69, p. 43,45
Chem.Abstr., 1950 , p. 1485
反应条件
1: 6.1 g / hydroxylamine hydrochloride / pyridine / 2 h / 100 °C 2: 2.9 g / LAH / diethyl ether View Scheme
参考文献
Nair, M. D.; David, J.; Nagarajan, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 940 - 947
反应条件
1: PPA (poliphosphoric acid) 2: N-bromosuccinimide (NBS) View Scheme
参考文献
Kukolja; Draheim; Pfeil; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 12 p. 1886 - 1896
反应条件
sodium tetrahydroborate
参考文献
Singh, Satwinder; Kumar, Subodh; Chimni, Swapandeep Singh
Enantiomer, 2002 , vol. 7, # 4-5 p. 231 - 240
反应条件
PPA (poliphosphoric acid)
参考文献
Matsunaga, Nobuyuki; Kaku, Tomohiro; Itoh, Fumio; Tanaka, Toshimasa; Hara, Takahito; Miki, Hiroshi; Iwasaki, Masahiko; Aono, Tetsuya; Yamaoka, Masuo; Kusaka, Masami; Tasaka, Akihiro
Bioorganic and medicinal chemistry, 2004 , vol. 12, # 9 p. 2251 - 2273
反应条件
aluminium trichloride in benzene 1.) benzene, 0 deg C, 0.5 h, 2.) reflux, 3 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 677 - 685