1-[(4-甲氧基苯基)硫基]丙酮合成路线 (共 5 条)
反应条件
pyridine T=100°C; 1 h;
参考文献
Carta, Antonio; Loriga, Mario; Paglietti, Giuseppe; Mattana, Antonella; Fiori, Pier Luigi; Mollicotti, Paola; Sechi, Leonardo; Zanetti, Stefania
European Journal of Medicinal Chemistry, 2004 , vol. 39, # 2 p. 195 - 203
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.25 h; 2: With sulfur in tetrahydrofuran; hexane T=-78°C; 3: chloroacetone in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Ham, Jungyeob; Yang, Inho; Kang, Heonjoong
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3236 - 3239
反应条件
potassium dihydrogenphosphate; tris-[2-carboxyethyl]-phosphine; human thiopurine S-methyltransferase; E. coli S-adenosylhomocysteine nucleosidase T=37°C; pH=8; Enzymatic reaction;
参考文献
Lee, Bobby W. K.; Sun, He G.; Zang, Tianzhu; Ju-Kim, Byung; Alfaro, Joshua F.; Zhou, Zhaohui Sunny
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3642 - 3643
反应条件
ethanol; sodium unter Kuehlung und anschliessendes Behandeln mit 1 Mol Chloraceton, zuletzt bei Siedetemperatur;
参考文献
Novelli; Zwaig
Anales de la Asociacion Quimica Argentina (1921-2001), 1944 , vol. 32, p. 89,91
参考文献
Banfield et al.
Journal of the Chemical Society, 1956 , p. 4791,4798