(3-羟基-3-苯基丙基)氨基甲酸叔丁酯合成路线 (共 12 条)
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; PdCl2(nbd) in toluene
T=80°C; P=760.051 Torr; 24 h; Title compound not separated from byproducts.;
参考文献
Caspi, Daniel D.; Ebner, David C.; Bagdanoff, Jeffrey T.; Stoltz, Brian M.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 2-3 p. 185 - 189
反应条件
oxygen; (-)-sparteine in toluene
T=80°C; P=760.051 Torr; 24 h; Molecular sieve; optical yield given as percent ee;
参考文献
Ebner, David C.; Bagdanoff, Jeffrey T.; Ferreira, Eric M.; McFadden, Ryan M.; Caspi, Daniel D.; Trend, Raissa M.; Stoltz, Brian M.
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 12978 - 12992