反应条件
1: 40 percent / 2.0 M phenyllithium / tetrahydrofuran; cyclohexane; diethyl ether / 2.33 h / -60 - -30 °C
2: pyridine / CH2Cl2 / 3 h / -20 °C
3: sodium azide / dimethylformamide / -20 °C
4: 95 percent / sodium borohydride / propan-2-ol / 48 h / Heating
5: 3-<(dimethylamino)propyl>-1-ethylcarbodiimide hydrochloride / CH2Cl2 / Ambient temperature
6: acetic acid / H2O / 45 °C
View Scheme
参考文献
Kiso, Makoto; Nakamura, Akemi; Tomita, Yoshimi; Hasegawa, Akira
Carbohydrate Research, 1986 , vol. 158, p. 101 - 112