1-(2-亚硝基苯基)-乙酮合成路线 （共 15 条）
反应条件
1: 95 percent / hydrazine hydrate, glacial acetic acid / ethanol; H2O / 3 h / Heating
2: MnO2 / CHCl3 / 0.08 h
3: CHCl3 / pH 4 - 5
4: H2O / Irradiation
View Scheme
参考文献
Walker, Jeffery W.; Reid, Gordon P.; McCray, James A.; Trentham, David R.
Journal of the American Chemical Society, 1988 , vol. 110, # 21 p. 7170 - 7177
反应条件
1: MnO2 / CHCl3 / 0.08 h
2: CHCl3 / pH 4 - 5
3: H2O / Irradiation
View Scheme
参考文献
Walker, Jeffery W.; Reid, Gordon P.; McCray, James A.; Trentham, David R.
Journal of the American Chemical Society, 1988 , vol. 110, # 21 p. 7170 - 7177
反应条件
2-[(2-Hydroxy-1,1-bis[hydroxymethyl]ethyl)amino]ethanesulfonic acid; potassium chloride; magnesium chloride
T=21°C; IrradiationpH 7.1; MechanismQuantum yieldRate constant;
参考文献
Walker, Jeffery W.; Reid, Gordon P.; McCray, James A.; Trentham, David R.
Journal of the American Chemical Society, 1988 , vol. 110, # 21 p. 7170 - 7177
反应条件
in water
Irradiation;
参考文献
Walker, Jeffery W.; Reid, Gordon P.; McCray, James A.; Trentham, David R.
Journal of the American Chemical Society, 1988 , vol. 110, # 21 p. 7170 - 7177
反应条件
in water
Irradiation;
参考文献
Walker, Jeffery W.; Reid, Gordon P.; McCray, James A.; Trentham, David R.
Journal of the American Chemical Society, 1988 , vol. 110, # 21 p. 7170 - 7177
反应条件
1: 62 percent / Et3N / tetrahydrofuran / -78 - 0 °C
2: tetrazole / acetonitrile
3: I2, pyridine, water / CH2Cl2
4: 56 percent / TFA / CH2Cl2
5: CDCl3 / 48 h / Irradiation
View Scheme
参考文献
Qiao, Lixin; Kozikowski, Alan P.; Olivera, Ana; Spiegel, Sarah
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 7 p. 711 - 714
反应条件
1: tetrazole / acetonitrile
2: I2, pyridine, water / CH2Cl2
3: 56 percent / TFA / CH2Cl2
4: CDCl3 / 48 h / Irradiation
View Scheme
参考文献
Qiao, Lixin; Kozikowski, Alan P.; Olivera, Ana; Spiegel, Sarah
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 7 p. 711 - 714
反应条件
dirhodium tetraacetate in tetrahydrofuran; water
Mechanism;
参考文献
Corrie; Reid
Journal of Labelled Compounds and Radiopharmaceuticals, 1995 , vol. 36, # 3 p. 289 - 300
反应条件
in chloroform-d1
48 h; Irradiation;
参考文献
Qiao, Lixin; Kozikowski, Alan P.; Olivera, Ana; Spiegel, Sarah
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 7 p. 711 - 714
反应条件
in acetonitrile
1.16667 h; UV-irradiation; Product distribution; Further Variations:irradiation wavelength;
参考文献
Serafinowski, Pawel J.; Garland, Peter B.
Journal of the American Chemical Society, 2003 , vol. 125, # 4 p. 962 - 965
