N-[3-(叔丁氧羰氨基)丙基]氨基乙酸乙酯合成路线 (共 4 条)
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=0 - 20°C; 4 h;
参考文献
Kurtan; Nesnas; Li; Huang; Nakanishi; Berova
Journal of the American Chemical Society, 2001 , vol. 123, # 25 p. 5962 - 5973
反应条件
1: 93 percent / tetrahydrofuran / 0 - 20 °C 2: 90 percent / DIPEA / tetrahydrofuran / 4 h / 0 - 20 °C View Scheme
参考文献
Kurtan; Nesnas; Li; Huang; Nakanishi; Berova
Journal of the American Chemical Society, 2001 , vol. 123, # 25 p. 5962 - 5973
反应条件
triethylamine; potassium iodide in dichloromethane T=40°C; 50 h;
参考文献
Shibata; Biplab Kumar Das; Honjo; Takeuchi
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 14 p. 1605 - 1611
反应条件
1: 98 percent / Et3N / CH2Cl2 / 11 h / 0 - 20 °C 2: 97 percent / aq. KOH / methanol / 2 h / 20 °C View Scheme
参考文献
Kurtan; Nesnas; Li; Huang; Nakanishi; Berova
Journal of the American Chemical Society, 2001 , vol. 123, # 25 p. 5962 - 5973