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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
25834-49-5
合成路线
（共 4 条）
25834-49-5
→
反应条件
32846-66-5
1,4-立方烷二羧酸
反应条件
1.1: sodium hydroxide / methanol / 3 h / |Reflux 2.1: sulfuric acid / 25 h / 20 - 25 °C 3.1: hydrogenchloride / methanol; water / 40 h / |Inert atmosphere; |Irradiation 3.2: 1.5 h / |Reflux; |Inert atmosphere 3.3: 4.5 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Beinat, Corinne; Banister, Samuel D.; Hoban, Jane; Tsanaktsidis, John; Metaxas, Athanasios; Windhorst, Albert D.; Kassiou, Michael
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 828 - 830
25834-49-5
→
反应条件
24539-28-4
4-甲氧羰基立方烷羧酸
反应条件
1.1: sodium hydroxide / methanol / 3 h / |Reflux 2.1: sulfuric acid / 25 h / 20 - 25 °C 3.1: hydrogenchloride / methanol; water / 40 h / |Inert atmosphere; |Irradiation 3.2: 1.5 h / |Reflux; |Inert atmosphere 3.3: 4.5 h / |Reflux; |Inert atmosphere 4.1: Dowex 50W-X8 resin / methanol / 24 h / |Reflux 5.1: sodium hydroxide / methanol; tetrahydrofuran / 14 h / 20 °C View Scheme
参考文献
Beinat, Corinne; Banister, Samuel D.; Hoban, Jane; Tsanaktsidis, John; Metaxas, Athanasios; Windhorst, Albert D.; Kassiou, Michael
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 828 - 830
25834-49-5
→
反应条件
32846-64-3
反应条件
1: sodium hydroxide / methanol / 3 h / |Reflux 2: sulfuric acid / 25 h / 20 - 25 °C View Scheme
参考文献
Beinat, Corinne; Banister, Samuel D.; Hoban, Jane; Tsanaktsidis, John; Metaxas, Athanasios; Windhorst, Albert D.; Kassiou, Michael
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 828 - 830
25834-49-5
→
反应条件
29412-62-2
1,4-立方烷二甲酸二甲酯
反应条件
1.1: sodium hydroxide / methanol / 3 h / |Reflux 2.1: sulfuric acid / 25 h / 20 - 25 °C 3.1: hydrogenchloride / methanol; water / 40 h / |Inert atmosphere; |Irradiation 3.2: 1.5 h / |Reflux; |Inert atmosphere 3.3: 4.5 h / |Reflux; |Inert atmosphere 4.1: Dowex 50W-X8 resin / methanol / 24 h / |Reflux View Scheme
参考文献
Beinat, Corinne; Banister, Samuel D.; Hoban, Jane; Tsanaktsidis, John; Metaxas, Athanasios; Windhorst, Albert D.; Kassiou, Michael
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 828 - 830
