N-甲基-4-硝基苯甲酰胺合成路线 （共 25 条）
反应条件
silica gel; caesium carbonate; 1-(toluene-p-sulphonyl)imidazole in N,N-dimethyl-formamide
Beckmann rearrangement; 2 h; Reflux;
参考文献
Rad, Mohammad Navid Soltani; Khalafi-Nezhad, Ali; Behrouz, Somayeh; Amini, Zohreh; Behrouz, Marzieh
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 8 p. 1658 - 1671
反应条件
silica gel; toluene-4-sulfonic acid
0.0333333 h; microwave irradiation;
参考文献
Hajipour; Ghasemi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 6 p. 504 - 507
反应条件
N-bromosuccinmide in chloroform
T=20°C; 18 h; Product distribution;
参考文献
Kuang, Liping; Zhou, Jing; Chen, Sheng; Ding, Ke
Synthesis, 2007 , # 20 p. 3129 - 3134
反应条件
tert-Butylisopropylthioketon
T=140°C;
参考文献
Schaumann,E.; Ehlers,J.
Chemische Berichte, 1979 , vol. 112, p. 1000 - 1011
参考文献
Salfetnikova; Vasil'ev; Rudenko
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 6 p. 838 - 844
反应条件
1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 25 °C
1.2: 8 h / 80 °C
2.1: trifluoroacetic acid; water / acetonitrile / 2 h / 80 °C / |Sealed tube
View Scheme
参考文献
Lee, Sang-Hak; Mu, Yu; Kim, Gun-Woo; Kim, Jin-Seok; Park, Seok-Hwi; Jin, Tian; Lee, Kee-Young; Ham, Won-Hun
Heterocycles, 2013 , vol. 87, # 8 p. 1749 - 1764
反应条件
in dichloromethane
72 h;
参考文献
Friedrichsen, Willy; Kujath, Eckard; Liebezeit, Gerd
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 2 p. 222 - 233
反应条件
sodium hydrogen sulphate; hydroxylamine hydrochloride; silica gel
0.0333333 h; Heating;
参考文献
Das; Ravindranath; Venkataiah; Madhusudhan
Journal of Chemical Research - Part S, 2000 , # 10 p. 482 - 483
反应条件
tert.-butylhydroperoxide; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in dichloromethane
T=30°C; Kinetics;
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
参考文献
Brady; Dunn
Journal of the Chemical Society, 1926 , p. 2414
