1-烯丙基嘧啶-2,4(1H,3H)-二酮合成路线 （共 4 条）
反应条件
1: [131I]-Uracil With sodium hydride; dimethyl sulfoxide T=20 - 60°C; 1 h; Inert atmosphere; 2: allyl bromide T=65°C; Inert atmosphereMicrowave irradiation;
参考文献
Sacarescu; Atudosie; Simionescu; Harabagiu
Chemistry of Heterocyclic Compounds, 2011 , vol. 47, # 5 p. 602 - 606
反应条件
palladium diacetate; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; 1,8-diazabicyclo[5.4.0]undec-7-ene in water; acetonitrile T=60°C; 24 h;
参考文献
Amblard, Franck; Nolan, Steven P.; Schinazi, Raymond F.; Agrofoglio, Luigi A.
Tetrahedron, 2005 , vol. 61, # 3 p. 537 - 544
反应条件
palladium diacetate; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; 1,8-diazabicyclo[5.4.0]undec-7-ene in water; acetonitrile T=60°C; 48 h;
参考文献
Goux, Catherine; Sigismondi, Silvana; Sinou, Denis; Perez, Montserrat; Moreno-Manas, Marcial; Pleixats, Roser; Villarroya, Merce
Tetrahedron, 1996 , vol. 52, # 28 p. 9521 - 9534
反应条件
in sodium hydroxide; acetone
参考文献
Tateoka; Kimura; Watanabe; Yamamoto; Ho
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 12 p. 4928 - 4934
