1-(4-甲基苯基)-3-苯基-1,3-丙烷二酮合成路线 （共 37 条）
反应条件
1: (i) NOHSO4, NaCl, (ii) /BRN= 1071236/, aq. NaOH
2: benzene / Irradiation
3: aq. HCl
View Scheme
参考文献
Giezendanner,H. et al.
Helvetica Chimica Acta, 1973 , vol. 56, p. 2588 - 2611
反应条件
1: (i) NOHSO4, NaCl, (ii) /BRN= 1071236/, aq. NaOH
2: benzene / Irradiation
3: aq. HCl
View Scheme
参考文献
Giezendanner,H. et al.
Helvetica Chimica Acta, 1973 , vol. 56, p. 2588 - 2611
反应条件
1: benzene / Irradiation
2: aq. HCl
View Scheme
参考文献
Giezendanner,H. et al.
Helvetica Chimica Acta, 1973 , vol. 56, p. 2588 - 2611
反应条件
1: Br2
2: NaOMe / methanol
View Scheme
参考文献
Dayer,F. et al.
Helvetica Chimica Acta, 1974 , vol. 57, # 7 p. 2201 - 2209
反应条件
sodium hydride in tetrahydrofuran; mineral oil
16.3333 h; Inert atmosphereReflux;
参考文献
Zhang, Hao; Feng, Dandan; Sheng, Haibo; Ma, Xuebing; Wan, Jinwei; Tang, Qian
RSC Advances, 2014 , vol. 4, # 13 p. 6417 - 6423
反应条件
1: 64 percent / nitromethane; CH2Cl2 / -50 deg C, 30 min to r.t., 18 h
2: 76 percent / HgCl2/HgO / methanol; H2O / 2 h / Heating
View Scheme
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 5 p. 1798 - 1808
参考文献
Giezendanner,H. et al.
Helvetica Chimica Acta, 1973 , vol. 56, p. 2588 - 2611
反应条件
2: glacial acetic acid / (Herstellung der stabilen Form vom F: 84grad)
View Scheme
参考文献
Weygand
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 112
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 178
反应条件
2: glacial acetic acid / (Herstellung der stabilen Form vom F: 84grad)
View Scheme
参考文献
Weygand
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 112
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 178
参考文献
Weygand
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 112
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 178
