反应条件
in tetrahydrofuran PhCH2Br was added dropwise to a THF soln. of Ni-complex at -78°C under Ar, mixt. was warmed slowly and allowed to react for 5 h; mixt. was poured onto solid iodine, stirred for 15 min, washed with aq. NaHSO3, aq. layers were washed with ether, ether ext. was combined with THF soln. and dried over K2CO3; BuC(O)CH2Ph was tentatively identified by GC-MS;
参考文献
Organometallics, , vol. 6, p. 1358 - 1360
