1,2,3,4,6-D-葡萄糖五乙酸酯合成路线 （共 84 条）
反应条件
pyridine; benzyl alcohol zinc salt 1.) CH2Cl2, reflux, 24 h, 2.) room temperature, 24 h; Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 24 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
pyridine; benzyl alcohol zinc salt 1.) CH2Cl2, reflux, 8 h, pyridine presence, 2.) room temperature, 24 h; Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
pyridine; sodium hydroxide; (NH4)2S2O8; potassium iodide 1.) 66.7 mM phosphate buffer, (pH 7.1), 60 deg C, 2 h, 2.) 50 deg C, 3.) 100 deg C, 2 h; Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 141, p. 77 - 90
反应条件
pyridine; sodium methylate; triethylamine 1.) AcOH, 5-7 deg C, 8 h, constant current electrolysis (Pt, 450 mA, 35-60 V); 2.) MeOH, 15 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 10 p. 3078 - 3086
反应条件
pyridine 1) Et2O, a) -20 deg C, 1 h, b) 0 deg C, 1 h, 2) r.t., overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 244, # 2 p. 275 - 284
反应条件
pyridine; sodium methylate; triethylamine 1.) AcOH, 5-7 deg C, 8 h, constant current electrolysis (Pt, 240 mA, 30-50 V); 2.) MeOH, 24 deg C, 30 min; 3.) 35 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 10 p. 3078 - 3086
反应条件
pyridine 1.) Bacillus circulans β-galactosidase presence, water, 2.) 20 deg C, 4 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 53, # 5 p. 1695 - 1706
反应条件
N(Et)4ClO4 in acetonitrile Arylation; ElectrolysisAg cathode; controlled potential; Further byproducts given;
参考文献
Physical Chemistry Chemical Physics, , vol. 1, # 12 p. 2989 - 2995
反应条件
sulfuric acid; acetic acid T=24°C; MechanismRate constant;
参考文献
Heterocycles, , vol. 35, # 1 p. 227 - 234
