1,2,3,4,6-D-葡萄糖五乙酸酯合成路线 (共 84 条)
反应条件
tin(IV) chloride in dichloromethane
T=20°C; 48 h;
参考文献
Kuehne, Marco; Gyoergydeak, Zoltan; Lindhorst, Thisbe K.
Synthesis, 2006 , # 6 p. 949 - 951
反应条件
1: phosphorus; bromine; acetic acid
2: anhydrous xylene / 0.42 h / 130 - 140 °C / Microwave irradiation
View Scheme
参考文献
Yadgire, Atul V.; Korpe, Gajanan V.; Deshmukh, Shirish P.
E-Journal of Chemistry, 2011 , vol. 8, # 4 p. 1614 - 1619
反应条件
indium trifluoromethanesulfonate in neat (no solvent)
1.5 h; Milling; stereospecific reaction;
参考文献
Kumar, Vajinder; Taxak, Nikhil; Jangir, Ramniwas; Bharatam, Prasad V.; Kartha, K. P. Ravindranathan
Journal of Organic Chemistry, 2014 , vol. 79, # 8 p. 3427 - 3439
反应条件
boron trifluoride diethyl etherate in nitromethane
T=35°C; 2 h;
参考文献
Lichtenthaler, Frieder W.; Nakamura, Katsumi; Klotz, Juergen
Angewandte Chemie - International Edition, 2003 , vol. 42, # 47 p. 5838 - 5843