1,1-二丁基-3-苯基脲合成路线 （共 18 条）
反应条件
oxygen; potassium iodide; PdI2 in ethylene glycol dimethyl ether T=100°C; P=15200 Torr; 15 h;
参考文献
Gabriele, Bartolo; Salerno, Giuseppe; Mancuso, Raffaella; Costa, Mirco
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4741 - 4750
反应条件
1: carbon monoxide; dibutylamine With selenium; sulfur in tetrahydrofuran T=20°C; Carbonylation; substitution; P=760 Torr; 24 h; 2: With methyl iodide in tetrahydrofuran T=20°C; Esterification; 3: [Li][NHPh] in tetrahydrofuran Substitution; Heating;
参考文献
Mizuno, Takumi; Kino, Takanobu; Takatoshi, Ito; Miyata, Toshiyuki
Synthetic Communications, 2000 , vol. 30, # 9 p. 1675 - 1688
反应条件
in toluene T=80°C; 1 h;
参考文献
Liu, Xiang Dong; Kimura, Mika; Sudo, Atsushi; Endo, Takeshi
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 23 p. 5298 - 5305
反应条件
selenium; triethylamine in toluene T=150 - 160°C; 1.5 h;
参考文献
Yang, Ying; Lu, Shiwei
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4845 - 4846
反应条件
in toluene T=150 - 160°C; Substitution; 2 h;
参考文献
Yang, Ying; Lu, Shiwei
Organic Preparations and Procedures International, 1999 , vol. 31, # 5 p. 559 - 561
反应条件
T=90°C; P=40 Torr; 1 h;
参考文献
Ma, Xiao-bo; Zhang, Jing-lin
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 227 - 231
参考文献
Societe Nationale des Poudres et Explosifs
Patent: US4709087 A1, 1987 ;
反应条件
zeolite HSZ-360 T=180°C; Condensation; 3 h;
参考文献
Bigi, Franca; Frullanti, Bettina; Maggi, Raimondo; Sartori, Giovanni; Zambonin, Elena
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 1004 - 1006
反应条件
1: 60 °C 2: dibutyl tin dilaurate / 1,2-dichloro-benzene / 70 °C View Scheme
参考文献
Dzalmukhanova; Lodygina; Komratova; Badamshina
Kinetics and Catalysis, 2013 , vol. 54, # 6 p. 656 - 661
Kinetika i Kataliz, 2013 , vol. 54, # 6 p. 696 - 701,6
反应条件
dibutyl tin dilaurate in 1,2-dichloro-benzene T=70°C; KineticsMechanismActivation energy; Concentration;
参考文献
Dzalmukhanova; Lodygina; Komratova; Badamshina
Kinetics and Catalysis, 2013 , vol. 54, # 6 p. 656 - 661
Kinetika i Kataliz, 2013 , vol. 54, # 6 p. 696 - 701,6
