5-甲基-2-(1-甲基乙烯基)-4-己烯-1-醇乙酸酯合成路线 （共 23 条）
反应条件
n-butylzinc chloride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
2 h; Heating; Title compound not separated from byproducts;
参考文献
Araki, Shuki; Kambe, Shinya; Kameda, Keiko; Hirashita, Tsunehisa
Synthesis, 2003 , # 5 p. 751 - 754
反应条件
methanesulfonic acid in nitromethane
T=0°C; 90 h;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene
T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
1: methanesulfonic acid / nitromethane / 90 h / 0 °C
2: phosphorus oxychloride / pyridine / Ambient temperature
View Scheme
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
反应条件
trichlorophosphate in pyridine
Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Julia, M.; Schmitz, C.
Tetrahedron, 1986 , vol. 42, # 9 p. 2485 - 2490
反应条件
pyridine in diethyl ether
cooling;
参考文献
Zada, Anat; Harel, Miriam
Tetrahedron Asymmetry, 2004 , vol. 15, # 15 p. 2339 - 2343
反应条件
pyridine; diethyl ether
acetate of natural levorotatory lavandulol;
参考文献
Schinz; Seidel
Helvetica Chimica Acta, 1942 , vol. 25, p. 1584
