4-(苯硫基)乙酰乙酸乙酯合成路线 （共 6 条）
反应条件
1: 63 percent / bakers' yeast, saccharose / aq. ethanol / 13 h 2: 85 percent / mCPBA 3: 68 percent / hydrogen / Raney-Ni (W4) / ethanol View Scheme
参考文献
Hayakawa, Ryuuichirou; Shimizu, Makoto; Fujisawa, Tamotsu
Tetrahedron Letters, 1996 , vol. 37, # 42 p. 7533 - 7536
反应条件
in ethanol 24 h; Heating; Yields of byproduct given;
参考文献
Sircar; Gregor; Anderson; Haleen; Shih; Weishaar; Steffen; Pugsley; Taylor
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2248 - 2260
反应条件
in 1,2-dichloro-ethane
T=50 - 60°C; 12 - 24 h;
参考文献
Gong, Ping; Zhao, Yanfang
Patent: US2008/249155 A1, 2008 ;
Location in patent: Page/Page column 19 ;
反应条件
1: 55 percent / potassium hydroxide / methanol / 7 h / Heating
2: 54 percent / phosphorus oxychloride / 9 h / 150 °C
View Scheme
参考文献
Sarkar, Tarun K.; Panda, Niranjan; Basak, Sankar
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6919 - 6927
反应条件
in ethanol
24 h; Heating; Yield given;
参考文献
Sircar; Gregor; Anderson; Haleen; Shih; Weishaar; Steffen; Pugsley; Taylor
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2248 - 2260
反应条件
in ethanol
24 h; Heating; Yield given;
参考文献
Sircar; Gregor; Anderson; Haleen; Shih; Weishaar; Steffen; Pugsley; Taylor
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2248 - 2260
