2-乙基磺酰基-1,3-苯并噻唑合成路线 （共 8 条）
反应条件
dihydrogen peroxide in acetic acid T=60 - 70°C; 4 h;
参考文献
Bourdon, Benjamin; Corbet, Matthieu; Fontaine, Patrice; Goekjian, Peter G.; Gueyrard, David
Tetrahedron Letters, 2008 , vol. 49, # 5 p. 747 - 749
反应条件
C30H51NOS; lithium hexamethyldisilazane in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Robiette, Raphael; Pospisil, Jiri
European Journal of Organic Chemistry, 2013 , # 5 p. 836 - 840
反应条件
1: aq. NaOH / ethanol / 40 - 60 °C 2: aq. H2O2 / acetic acid / 4 h / 60 - 70 °C View Scheme
参考文献
Kuznetsova,E.A. et al.
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, p. 767 - 772,769 - 773
反应条件
hydrogen; PdCl2/C in ethanol
参考文献
Kuznetsova,E.A. et al.
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, p. 767 - 772,769 - 773
反应条件
1: Al2O3 / benzene 2: H2 / PdCl2-C / ethanol View Scheme
参考文献
Zhurnal Organicheskoi Khimii, , vol. 1, p. 767 - 772,769 - 773
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane -78 deg C, 3 h then rt., 1 h;
参考文献
Baudin, J. B.; Hareau, G.; Julia, S. A.; Lorne, R.; Ruel, O.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 856 - 878
反应条件
tetrabutyl ammonium fluoride 1) electrolysis, DMF; Yield given. Multistep reaction;
参考文献
Delaunay; Mabon; Chaquiq El Badre; Orliac; Simonet
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2149 - 2150
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane
-78 deg C, 3 h then rt., 1 h;
参考文献
Baudin, J. B.; Hareau, G.; Julia, S. A.; Lorne, R.; Ruel, O.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 856 - 878
