4-氟-4'-羟基二苯甲酮合成路线 （共 10 条）
反应条件
tri-tert-butyl phosphine; potassium carbonate; acetone; [Rh(C2H4)2Cl]2 in 1,4-dioxane; toluene T=20 - 80°C;
参考文献
Mora, Guilhem; Darses, Sylvain; Genet, Jean-Pierre
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1180 - 1184
反应条件
hydrogenchloride; trifluoroacetic anhydride; aluminium chloride in o-di-fluorobenzene; dichloromethane; water
反应条件
potassium hydroxide in water; dimethyl sulfoxide T=60°C; 18 h;
参考文献
Ridd, John H.; Yousaf, Taher I.; Rose, John B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1729 - 1734
参考文献
Pest Management Science, , vol. 57, # 2 p. 191 - 202
反应条件
1.1: AlCl3 / nitrobenzene / 0.17 h / 0 - 8 °C 1.2: nitrobenzene / 6 - 20 °C 2.1: aq. HBr; AcOH / 5 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 15 p. 3354 - 3370
反应条件
1.1: AlCl3 / nitrobenzene / 0.17 h / 0 - 8 °C 1.2: nitrobenzene / 6 - 20 °C 2.1: aq. HBr; AcOH / 5 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 15 p. 3354 - 3370
反应条件
aluminium trichloride
参考文献
FR2300552DE2605382 , ;
Chem.Abstr., , vol. 85, # 192382
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 6 h;
参考文献
Suzuki, Yukimitsu; Hiraoka, Shuichi; Yokoyama, Akihiro; Yokozawa, Tsutomu
Macromolecules, 2003 , vol. 36, # 13 p. 4756 - 4765
反应条件
1: KOH / methanol; H2O 2: 52 percent / dimethylsulfoxide / 70 - 80 °C View Scheme
参考文献
Ridd, John H.; Yousaf, Taher I.; Rose, John B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1729 - 1734
反应条件
1: KOH / methanol; H2O
2: 52 percent / dimethylsulfoxide / 70 - 80 °C
3: KOH / H2O; dimethylsulfoxide / 18 h / 60 °C
View Scheme
参考文献
Ridd, John H.; Yousaf, Taher I.; Rose, John B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1729 - 1734
