4-(乙酰基氧基)-6,8-二甲氧基-2-萘羧酸乙酯合成路线 （共 7 条）
反应条件
1: t-BuOK / 2-methyl-propan-2-ol / 2 h / Heating 2: 8.10 g / sodium acetate / 2 h / 140 °C View Scheme
参考文献
Pillay, Adushan; Rousseau, Amanda L.; Fernandes, Manuel A.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 38 p. 7809 - 7819
反应条件
potassium acetate 2 h; Heating;
参考文献
Kraus, George A; Ogutu, Herbert
Tetrahedron, 2002 , vol. 58, # 37 p. 7391 - 7395
反应条件
sodium acetate T=140°C; 2 h;
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
acetic anhydride 3 h; Reflux;
参考文献
Pillay, Adushan; Rousseau, Amanda L.; Fernandes, Manuel A.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 38 p. 7809 - 7819
反应条件
(i) KOtBu, (ii) /BRN= 3595639/, Ac2O; Multistep reaction;
参考文献
Harper,S.H. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , vol. <C>, p. 626 - 636
反应条件
acetyl chloride in methanol
T=0 - 20°C; 12 h;
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
1: 95 percent / guanidine hydrochloride; t-BuOK / ethanol; CH2Cl2 / 1.5 h / 20 °C
2: 99 percent / K2CO3 / acetone / 16 h / Heating
View Scheme
参考文献
Kraus, George A; Ogutu, Herbert
Tetrahedron, 2002 , vol. 58, # 37 p. 7391 - 7395
