n-n-丁基氨基甲酸甲酯合成路线 （共 27 条）
反应条件
nitric acid T=0°C; man giesst das Reaktionsprodukt auf ein Gemisch von Eis und Sodakrystallen;
参考文献
White,E.H. et al.
Journal of Organic Chemistry, 1966 , vol. 31, p. 3038 - 3046
反应条件
4-(N,N-dimethlyamino)pyridine in anhydrous xylene
参考文献
BASF Aktiengesellschaft
Patent: US5639890 A1, 1997 ;
反应条件
boron trichloride; triethylamine in benzene 0.5 h; Heating;
参考文献
Chemical Communications, , # 23 p. 2575 - 2576
反应条件
oxygen; copper-(N-heterocyclic carbene) complex
T=100°C; P=37503.8 Torr; 3 h;
参考文献
Zheng, Shuzhan; Li, Fuwei; Liu, Jianming; Xia, Chungu
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5883 - 5886
反应条件
yttria-zirconia based Lewis acid catalyst in acetonitrile
T=20°C; 0.0833333 h;
参考文献
Pandey, Rajesh K.; Dagade, Sharda P.; Dongare, Mohan K.; Kumar, Pradeep
Synthetic Communications, 2003 , vol. 33, # 23 p. 4019 - 4027
反应条件
silica gel immobilized lanthanum in toluene
T=120°C; AutoclaveInert atmosphere; chemoselective reaction;
参考文献
Guo, Xiaoguanga; Shang, Jianpenga; Li, Jiana; Wang, Liguoa; Ma, Yuboa; Shi, Feng; Deng, Youquan
Chinese Journal of Chemistry, 2010 , vol. 28, # 2 p. 164 - 170
反应条件
in tetrahydrofuran
T=50°C; 0.5 h;
参考文献
Giannoccaro, Potenzo; Tommasi, Immacolata; Aresta, Michele
Journal of Organometallic Chemistry, 1994 , vol. 476, # 1 p. 13 - 18
反应条件
carbon monoxide; triphenylphosphine in methanol
Cu-compd. in MeOH satd. with CO, is allowed to react with 1 atm of CO at 70°C as the green colour lightened (about 4 h). Cooling of reactor to 22°C and measuring of volume of unreacted CO.; IR and MS identification of org. compd., GLC anal.; detn. of Cu(I) present in soln. after addn. of PPh3, elem. anal.;
参考文献
Giannoccaro, Potenzo
Journal of Organometallic Chemistry, 1994 , vol. 470, # 1.2 p. 249 - 252
参考文献
Halcon Research and Development Corp.
Patent: US4258201 A1, 1981 ;
反应条件
1-butyl-3-methyl imidazole hydrochloride
T=170°C; 1 h;
参考文献
Sima, Tianlong; Guo, Shu; Shi, Feng; Deng, Youquan
Tetrahedron Letters, 2002 , vol. 43, # 45 p. 8145 - 8147
