n-n-丁基氨基甲酸甲酯合成路线 （共 27 条）
反应条件
water; sodium acetate
1.) anodic oxidation, AcOH,; Multistep reaction;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Onomura, Osamu; Kanazawa, Takenobu; Habuka, Masahiro
Chemistry Letters, 1984 , p. 1101 - 1104
反应条件
in N,N-dimethyl-formamide
参考文献
Singh, Krishna Nand
Synthetic Communications, 2007 , vol. 37, # 16 p. 2651 - 2654
反应条件
1.) 0 deg C, 2 h, 2.) THF; Yield given. Multistep reaction;
参考文献
Giannoccaro, Potenzo; Ravasio, Nicoletta; Aresta, Michele
Journal of Organometallic Chemistry, 1993 , vol. 451, # 1.2 p. 243 - 248
反应条件
in 1,2-dichloro-ethane
T=28°C;
参考文献
Berlin, P. A.; Tiger, R. P.; Filippova, I. S.; Levina, M. A.; Dzhaparidze, N. N.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 9.2. p. 2140 - 2147,1909 - 1915
参考文献
Junod
Helvetica Chimica Acta, 1952 , vol. 35, p. 1667,1673
反应条件
(i) LiAlH4, Et2O, (ii) /BRN= 506104/; Multistep reaction;
参考文献
Holland,H.L.; Johnson,G.B.
Tetrahedron Letters, 1979 , p. 3395 - 3396
反应条件
1.1: NaH / dimethylformamide / 2 h / 60 °C
1.2: 76 percent / dimethylformamide / 14.5 h / 60 °C
2.1: Bu4NBF4; trifluoromethanesulfonic acid / CH2Cl2 / -78 °C / Electrolysis; anodic oxidation
3.1: CH2Cl2 / -78 °C
View Scheme
参考文献
Suga, Seiji; Nagaki, Aiichiro; Yoshida, Jun-Icih
Chemical Communications, 2003 , # 3 p. 354 - 355
