2-[N-甲基-N-(5-硝基-2-吡啶基)氨基]乙醇合成路线 (共 3 条)
参考文献
Gruenenthal GmbH; FRANK, Robert; Christoph, Thomas; Lesch, Bernhard; Lee, Jeewoo
Patent: US2013/29961 A1, 2013 ;
Location in patent: Paragraph 0739 ;
反应条件
triethylamine in dichloromethane T=23°C; 3 h;
参考文献
Takahashi, Eiki; Hirano, Noriyuki; Nagahara, Takashi; Yoshikawa, Satoru; Momen, Shinobu; Yokokawa, Hiroshi; Hayashi, Ryoji
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3154 - 3156
反应条件
1: trichlorophosphate; phosphorus pentachloride / 16 h / 60 °C 2: 1 h / 23 °C View Scheme
参考文献
Gruenenthal GmbH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: US2013/29962 A1, 2013 ;