烯丙基-beta-吡喃半乳糖苷合成路线 (共 19 条)
反应条件
sodium methylate in methanol 10 h;
参考文献
Binder, W. H.; Schmid, W.
Monatshefte fuer Chemie, 1995 , vol. 126, # 8.9 p. 923 - 932
反应条件
Dowex 50-X2-100 (H+) 1.5 h; Heating;
参考文献
Jenkins, David J.; Potter, Barry V.L.
Carbohydrate Research, 1996 , vol. 287, # 2 p. 169 - 182
反应条件
1: tin(IV) chloride / CH2Cl2 / 0.75 h / 20 °C 2: Et3N; H2O / methanol / 24 h / 20 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 42, # 3 p. 666 - 669
反应条件
immobilized β-D-glucosidase T=50°C; 72 h;
参考文献
Kishida, Masashi; Akita, Hiroyuki
Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
反应条件
1: Ag2CO3 / 4A molecular sieves / CH2Cl2 / 60 h / Ambient temperature 2: K2CO3 / methanol / 4.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 52, # 22 p. 7663 - 7678
反应条件
water; almond β-glucosidase T=50°C;
参考文献
Csuk, Rene; Prell, Erik; Korb, Claudia; Kluge, Ralph; Stroehl, Dieter
Tetrahedron, 2010 , vol. 66, # 2 p. 467 - 472
反应条件
hydrogenchloride T=70°C; 4.5 h;
参考文献
Macromolecules, , vol. 36, # 7 p. 2441 - 2447
反应条件
gold(III) chloride in acetonitrile 4 h; RefluxInert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 21 p. 8417 - 8420
反应条件
1.1: silver(l) oxide / diethyl ether / |Inert atmosphere 2.1: sodium / methanol / |Inert atmosphere; |Reflux 2.2: Dowex 50 Χ 8 resin / |Inert atmosphere; |Cooling View Scheme
参考文献
Organic Process Research and Development, , vol. 4, # 1 p. 34 - 42
反应条件
trifluoroacetic acid T=105°C; 26 h;
参考文献
Carbohydrate Research, , vol. 342, # 2 p. 217 - 235