3,5-二溴-4-羟基苯甲醛肟合成路线 (共 4 条)
反应条件
pyridine; hydroxylamine hydrochloride in methanol T=20°C; 24 h;
参考文献
Garcia-Alvarez, Rocio; Diaz-Alvarez, Alba E.; Borge, Javier; Crochet, Pascale; Cadierno, Victorio
Organometallics, 2012 , vol. 31, # 17 p. 6482 - 6490
反应条件
[RuCl2(η2-C6H6){P(NMe2)3}]; water T=100°C; 7 h; Inert atmosphereSealed tube;
参考文献
Garcia-Alvarez, Rocio; Diaz-Alvarez, Alba E.; Borge, Javier; Crochet, Pascale; Cadierno, Victorio
Organometallics, 2012 , vol. 31, # 17 p. 6482 - 6490
反应条件
sodium ethanolate in ethanol; acetonitrile
参考文献
Ciba-Geigy
Patent: US3941832 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 5159
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Ciba-Geigy
Patent: US3941839 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 5160
反应条件
trifluoromethylsulfonic anhydride; triethylamine; triphenylphosphine in dichloromethane T=0°C; 0.166667 h;
参考文献
Moussa, Ziad; Ahmed, Saleh A.; ElDouhaibi, Ahmad S.; Al-Raqa, Shaya Y.
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1826 - 1831