2-甲氧基-4-硝基苯甲酸合成路线 (共 33 条)
反应条件
1: With sodium hydroxide in methanol; water T=60°C; 0.5 h; 2: With hydrogenchloride in methanol; water
参考文献
Fukai, Ryosuke; Zheng, Xiaoxia; Motoshima, Kazunori; Tai, Akihiro; Yazama, Futoshi; Kakuta, Hiroki
ChemMedChem, 2011 , vol. 6, # 3 p. 550 - 560
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 16 h; Inert atmosphere;
参考文献
Adler, Marc J.; Hamilton, Andrew D.
Journal of Organic Chemistry, 2011 , vol. 76, # 17 p. 7040 - 7047
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Fukai, Ryosuke; Zheng, Xiaoxia; Motoshima, Kazunori; Tai, Akihiro; Yazama, Futoshi; Kakuta, Hiroki
ChemMedChem, 2011 , vol. 6, # 3 p. 550 - 560
反应条件
sulfuric acid anschliessendes Erwaermen mit wss. NaNO2;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 592,595
反应条件
sulfuric acid; nitric acid; acetic anhydride T=-8 - -5°C;
参考文献
Journal of the Chemical Society, , vol. 121, p. 1656
反应条件
potassium carbonate; N,N-dimethyl-formamide T=140°C;
参考文献
Journal of Fluorine Chemistry, , vol. 128, # 12 p. 1461 - 1468
反应条件
1: potassium carbonate / N,N-dimethyl-formamide 2: sodium hydroxide; water / tetrahydrofuran / Reflux View Scheme
反应条件
potassium permanganate
参考文献
Helvetica Chimica Acta, , vol. 24, p. 30,37
反应条件
1: nitric acid / nachfolgend Verseifung mit Salzsaeure 2: Diazotization View Scheme
参考文献
Journal of the Chemical Society, , vol. 111, p. 232
反应条件
1: ZnCl2; petroleum ether; HCl / 75 °C View Scheme
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 196, p. 1411
Bulletin de la Societe Chimique de France, , vol. <5> 1, p. 539,545