N-[2-[(2-溴-4,6-二硝基苯基)偶氮]-5-[(2-羟基乙基)氨基]-4-甲氧基苯基]-乙酰胺合成路线 （共 4 条）
反应条件
1.1: p-TSA / benzene / 3 h / Heating 2.1: 5 h / 80 °C 3.1: 9.54 g / H2O / 1 h / 100 °C 4.1: K2CO3 / CH2Cl2 / 1 h / 20 °C 5.1: H2 / 5 percent Pd/C / ethyl acetate 6.1: K2CO3 / ethyl acetate / 1 h 7.1: 670 mg / K2CO3; MeOH / 2 h / 0 °C 8.1: NaNO2; H2SO4 8.2: 85 percent / H2SO4 View Scheme
参考文献
Shiozawa, Tatsushi; Tada, Atsuko; Nukaya, Haruo; Watanabe, Tetsushi; Takahashi, Yoshifumi; Asanoma, Masaharu; Ohe, Takeshi; Sawanishi, Hiroyuki; Katsuhara, Taka; Sugimura, Takashi; Wakabayashi, Keiji; Terao, Yoshiyasu
Chemical Research in Toxicology, 2000 , vol. 13, # 7 p. 535 - 540
反应条件
1.1: 5 h / 80 °C 2.1: 9.54 g / H2O / 1 h / 100 °C 3.1: K2CO3 / CH2Cl2 / 1 h / 20 °C 4.1: H2 / 5 percent Pd/C / ethyl acetate 5.1: K2CO3 / ethyl acetate / 1 h 6.1: 670 mg / K2CO3; MeOH / 2 h / 0 °C 7.1: NaNO2; H2SO4 7.2: 85 percent / H2SO4 View Scheme
参考文献
Shiozawa, Tatsushi; Tada, Atsuko; Nukaya, Haruo; Watanabe, Tetsushi; Takahashi, Yoshifumi; Asanoma, Masaharu; Ohe, Takeshi; Sawanishi, Hiroyuki; Katsuhara, Taka; Sugimura, Takashi; Wakabayashi, Keiji; Terao, Yoshiyasu
Chemical Research in Toxicology, 2000 , vol. 13, # 7 p. 535 - 540
反应条件
1.1: K2CO3 / CH2Cl2 / 1 h / 20 °C 2.1: H2 / 5 percent Pd/C / ethyl acetate 3.1: K2CO3 / ethyl acetate / 1 h 4.1: 670 mg / K2CO3; MeOH / 2 h / 0 °C 5.1: NaNO2; H2SO4 5.2: 85 percent / H2SO4 View Scheme
参考文献
Shiozawa, Tatsushi; Tada, Atsuko; Nukaya, Haruo; Watanabe, Tetsushi; Takahashi, Yoshifumi; Asanoma, Masaharu; Ohe, Takeshi; Sawanishi, Hiroyuki; Katsuhara, Taka; Sugimura, Takashi; Wakabayashi, Keiji; Terao, Yoshiyasu
Chemical Research in Toxicology, 2000 , vol. 13, # 7 p. 535 - 540
反应条件
1: 2,4-dinitro-6-bromo-aniline With sulfuric acid; sodium nitrite 2: 3-[(2-hydroxyethyl)amino]-4-methoxyacetanilide With sulfuric acid
参考文献
Shiozawa, Tatsushi; Tada, Atsuko; Nukaya, Haruo; Watanabe, Tetsushi; Takahashi, Yoshifumi; Asanoma, Masaharu; Ohe, Takeshi; Sawanishi, Hiroyuki; Katsuhara, Taka; Sugimura, Takashi; Wakabayashi, Keiji; Terao, Yoshiyasu
Chemical Research in Toxicology, 2000 , vol. 13, # 7 p. 535 - 540
