2,3,5,6-四甲基苯甲酸合成路线 （共 21 条）
参考文献
Fuson et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4858
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-30°C; Inert atmosphereReflux;
参考文献
Mugridge, Jeffrey S.; Bergman, Robert G.; Raymond, Kenneth N.
Journal of the American Chemical Society, 2011 , vol. 133, # 29 p. 11205 - 11212
反应条件
Nafion-H in toluene T=100°C; 12 h;
参考文献
Olah, George A.; Laali, Khosrow; Mehrotra, Ashok K.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3360 - 3362
参考文献
Jacobsen
Chemische Berichte, 1889 , vol. 22, p. 1217
参考文献
Klages; Lickroth
Chemische Berichte, 1899 , vol. 32, p. 1563
反应条件
nitric acid; acetic anhydride; sodium carbonate 1.) 0 deg C, 2 h, 2.) 0 deg C to RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Keumi, Takashi; Morita, Toshio; Teramoto, Koichi; Takahashi, Hisakazu; Yamamoto, Hiroshi; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3439 - 3446
参考文献
Fuson et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4858
反应条件
Pb(II) thiocyanate
T=200 - 230°C;
参考文献
Rudenko; Salfetnikova; Vasil'ev
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 10 p. 1447 - 1470
反应条件
1: thionyl chloride
2: AlCl3; carbon disulfide / 60 °C
View Scheme
参考文献
Coops et al.
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 1109,1111
参考文献
Moffett, Robert Bruce
Journal of Chemical and Engineering Data, 1980 , vol. 25, # 2 p. 176 - 183
