1-甲氧基-4-(1-苯基乙基)-苯合成路线 (共 39 条)
反应条件
(C6H5CON2C3H(CF3)2O)Ni(II)(tris(4-dimethylamino)pyridine) in tetrahydrofuran
T=70°C; 24 h; Inert atmosphere;
参考文献
Someya, Chika I.; Inoue, Shigeyoshi; Krackl, Sebastian; Irran, Elisabeth; Enthaler, Stephan
European Journal of Inorganic Chemistry, 2012 , # 8 p. 1269 - 1277
反应条件
1-(N,N-dimethylamino)pyrene; triethylamine in acetonitrile
T=20°C; Irradiation;
参考文献
Penner, Alexander; Baetzner, Effi; Wagenknecht, Hans-Achim
Synlett, 2012 , vol. 23, # 19 p. 2803 - 2807
参考文献
Burtner; Brown
Journal of the American Chemical Society, 1953 , vol. 75, p. 2334,2337
反应条件
digallium tetrachloride in carbon disulfide
24 h; Heating;
参考文献
Hashimoto; Hirata; Kihara; Hasegawa; Saigo
Tetrahedron Letters, 1992 , vol. 33, # 42 p. 6351 - 6354
反应条件
potassium carbonate in pyridine
12 h; Inert atmosphereReflux;
参考文献
Li, Xijing; Feng, Yuanyuan; Lin, Lin; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 23 p. 10991 - 10995
反应条件
anhydrous iron chloride in 1,2-dichloro-ethane
T=20°C; Friedel-Crafts Alkylation; 3 h; Inert atmosphere; Overall yield = 95 percent; regioselective reaction;
参考文献
Sawama, Yoshinari; Shishido, Yuko; Kawajiri, Takahiro; Goto, Ryota; Monguchi, Yasunari; Sajiki, Hironao
Chemistry - A European Journal, 2014 , vol. 20, # 2 p. 510 - 516
反应条件
digallium tetrachloride in carbon disulfide
24 h; Heating; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
1: p-TsOH / benzene / Heating
2: CaY zeolite / hexane / 3 h / Ambient temperature
View Scheme
参考文献
Kao, Hsien-Ming; Grey, Clare P.; Pitchumani, Kasi; Lakshminarasimhan; Ramamurthy
Journal of Physical Chemistry A, 1998 , vol. 102, # 28 p. 5627 - 5638
反应条件
CaY zeolite in hexane
3 h; Ambient temperature; Yield givenYields of byproduct given;
参考文献
Kao, Hsien-Ming; Grey, Clare P.; Pitchumani, Kasi; Lakshminarasimhan; Ramamurthy
Journal of Physical Chemistry A, 1998 , vol. 102, # 28 p. 5627 - 5638
反应条件
1: tetrahydrofuran; diethyl ether / 21 h / 0 - 20 °C / Inert atmosphere
2: n-heptane; 1,2-dichloro-ethane / 16 h / 50 °C
View Scheme
参考文献
Mahoney, Stuart J.; Lou, Tiantong; Bondarenko, Ganna; Fillion, Eric
Organic Letters, 2012 , vol. 14, # 13 p. 3474 - 3477