N-氧代-N,N-二甲基-1-辛胺合成路线 (共 2 条)
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Caliskan, Hafize; Zaim, Oemer
Synthetic Communications, 2010 , vol. 40, # 20 p. 3078 - 3083
反应条件
dihydrogen peroxide; benzonitrile; Mg-Al-O-t-Bu HT (Catalyst B) in methanol; water
T=65°C; 0.5 h; Product distribution / selectivity;
参考文献
Council of Scientific and Industrial Research
Patent: EP1348692 A1, 2003 ;
Location in patent: Page/Page column 7 ;