顺-1,2-环丁二甲酯(CBDE)合成路线 （共 12 条）
参考文献
Martin-Vila, Marta; Muray, Elena; Aguado, Gemma P.; Alvarez-Larena, Angel; Branchadell, Vicenc; Minguillon, Cristina; Giralt, Ernest; Ortuo, Rosa M.
Tetrahedron Asymmetry, 2000 , vol. 11, # 17 p. 3569 - 3584
反应条件
5 Pd(II)/C(eggshell); hydrogen; triethylamine in ethanol
T=20°C; P=4560.31 Torr; 58 h;
参考文献
Torres, Elisabeth; Gorrea, Esther; Burusco, Kepa K.; Da Silva, Eric; Nolis, Pau; Rua, Federico; Boussert, Stephanie; Diez-Perez, Ismael; Dannenberg, Samantha; Izquierdo, Sandra; Giralt, Ernest; Jaime, Carlos; Branchadell, Vicen; Ortuno, Rosa M.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 3 p. 564 - 575
反应条件
hydrogen; triethylamine; palladium on activated charcoal
参考文献
van Tamelen,E.E.; Carty,D.
Journal of the American Chemical Society, 1971 , vol. 93, # 23 p. 6102 - 6110
反应条件
bis(triphenylphosphine)(.eta.(2)-ethylene)nickel(0) in toluene
T=17°C; 46 h; Irradiation;
参考文献
Miyashita, Akira; Ikezu, Shohgo; Nohira, Hiroyuki
Chemistry Letters, 1985 , p. 1235 - 1238
反应条件
sulfuric acid
Heating;
参考文献
Martin-Vila, Marta; Minguillon, Cristina; Ortuno, Rosa M.
Tetrahedron Asymmetry, 1998 , vol. 9, # 24 p. 4291 - 4294
反应条件
tetra-n-butylammonium perchlorate; sodium iodide in N,N-dimethyl-formamide
electrolysis: Pt cathode, Cu anode; Yield given. Yields of byproduct given;
参考文献
Tokuda, Masao; Hayashi, Atsushi; Suginome, Hiroshi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2590 - 2592
反应条件
1: (CF3CO)2O
2: methanol
View Scheme
参考文献
Schneider, Manfred; Engel, Norbert; Hoenicke, Petra; Heinemann, Gerd; Goerisch, Helmut
Angewandte Chemie, 1984 , vol. 96, # 1 p. 55 - 56
参考文献
Mohr, Peter; Waespe-Sarcevic, Nada; Tamm, Christoph; Gawronska, Krystyna; Gawronsky, Jacek K.
Helvetica Chimica Acta, 1983 , vol. 66, # 8 p. 2501 - 2511
反应条件
nitric acid
1.) 3.5 h, heating on a steam-bath, 2.) ether; Multistep reaction;
参考文献
Bryce-Smith, Derek; Foulger, Brian; Forrester, John; Gilbert, Andrew; Orger, Brian H.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 55 - 71
参考文献
Schneider, Manfred; Engel, Norbert; Hoenicke, Petra; Heinemann, Gerd; Goerisch, Helmut
Angewandte Chemie, 1984 , vol. 96, # 1 p. 55 - 56
