2-(氯甲氧基)-1,1,1,3,3,3-六氟丙烷合成路线 (共 14 条)
反应条件
water T=90°C; 1.5 h; Product distribution / selectivity;
参考文献
MINRAD INC.
Patent: WO2006/55748 A2, 2006 ;
Location in patent: Page/Page column 7 ;
反应条件
sulfuric acid; water 18 h; Heating / reflux; Conversion of starting material;
参考文献
Baxter International Inc
Patent: US2004/147779 A1, 2004 ;
Location in patent: Page 4,5 ;
反应条件
diisopropylethylamine hydrofluoride 16 h; Heating;
参考文献
Kudzma; Huang; Lessor; Rozov; Afrin; Kallashi; McCutcheon; Ramig
Journal of Fluorine Chemistry, 2001 , vol. 111, # 1 p. 11 - 16
反应条件
hydrogenchloride; potassium fluoride; water; Aliquat HTA-1 T=100°C; 3 h; Product distribution / selectivity;
参考文献
MINRAD INC.
Patent: WO2006/55748 A2, 2006 ;
Location in patent: Page/Page column 13 ;